The Synthesis and Characterization of bis(3-phenyldithio carbazato) lead(II): A New Single-source Precursor, Designed for Growth of PbS Nanocompounds
Metal complex of the type ML2 [M = Pb; L = 3-phenyldithiocarbazate] have been synthesized and characterized by UV-vis and FT-IR spectroscopy. The complex is formulated as four coordinate species where dithiocarbazate acting as bidentate chelating ligand. The complex, which is used as precursors, thermolysed in ethylene glycol to achieved single crystalline PbS nanocompounds without using any surfactant and additives under mild reaction condition. The nanocompounds are confirmed by TEM and FL spectroscopic analysis.
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