The Synthesis and Characterization of bis(3-phenyldithio carbazato) lead(II): A New Single-source Precursor, Designed for Growth of PbS Nanocompounds

  • Nilkamal Maiti

Abstract

Metal complex of the type ML2 [M = Pb; L = 3-phenyldithiocarbazate] have been synthesized and characterized by UV-vis and FT-IR spectroscopy. The complex is formulated as four coordinate species where dithiocarbazate acting as bidentate chelating ligand. The complex, which is used as precursors, thermolysed in ethylene glycol to achieved single crystalline PbS nanocompounds without using any surfactant and additives under mild reaction condition. The nanocompounds are confirmed by TEM and FL spectroscopic analysis.

Published
2017-05-09
How to Cite
MAITI, Nilkamal. The Synthesis and Characterization of bis(3-phenyldithio carbazato) lead(II): A New Single-source Precursor, Designed for Growth of PbS Nanocompounds. ADVANCED JOURNAL OF BASIC AND APPLIED SCIENCES, [S.l.], v. 1, n. 1, p. 12, may 2017. Available at: <http://ajbas.in/ojs/index.php/ajbas/article/view/2>. Date accessed: 24 sep. 2017.